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Simplified approach for the extraction of quinclorac from soils

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成果类型:
期刊论文
作者:
Wang, Yan-Hui;Li, Xin;Zhou, Xiao-Mao;Bai, Lian-Yang*
通讯作者:
Bai, Lian-Yang
作者机构:
[Bai, Lian-Yang; Wang, Yan-Hui; Li, Xin; Zhou, Xiao-Mao] Hunan Agr Univ, Inst Pesticide Sci, Changsha 410128, Hunan, Peoples R China.
[Bai, Lian-Yang] Hunan Inst Humanities Sci & Technol, Loudi 417000, Peoples R China.
通讯机构:
[Bai, Lian-Yang] H
Hunan Agr Univ, Inst Pesticide Sci, Changsha 410128, Hunan, Peoples R China.
语种:
英文
关键词:
QuEChERS;Quinclorac;Soil
期刊:
Asian Journal of Chemistry
ISSN:
0970-7077
年:
2012
卷:
24
期:
5
页码:
2042-2044
基金类别:
National Natural Foundation of ChinaNational Natural Science Foundation of China (NSFC) [30971936, 31071716]
机构署名:
本校为第一且通讯机构
院系归属:
植物保护学院
摘要:
A simplified version of the QuEChERS method for the extraction of quinclorac from soil samples was proposed. Optimum results were obtained dispersing soil in water, followed by the addition of 1 % acetic acid in acetonitrile, magnesium sulfate and sodium acetate as a modification of the quick, easy, cheap, effective, rugged and safe (QuEChERS) method. Liquid chromatography/ultraviolet (LC-UV) detector was then used to analyze the extracts without any other sample pretreatment. The result showed the recovery ranged from 73.8 to 106.4 % and 66.6 to 87.3 % with the relative standard deviations of...

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