TBAI-catalyzed selective synthesis of sulfonamides and β-aryl sulfonyl enamines: coupling of arenesulfonyl chlorides and sodium sulfinates with tert-amines

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成果类型：

期刊论文

作者：

Jiang, Hongmei;Tang, Xiaoyue;Xu, Zhihui;Wang, Huixian;Han, Kang;...

通讯作者：

Gui, Qingwen

作者机构：

[Zhou, Yuanyuan; Han, Kang; Tang, Xiaoyue; Yang, Xiaolan; Gui, Qingwen; Wang, Huixian; Feng, Yong-Lai; Jiang, Hongmei] Hunan Agr Univ, Coll Sci, Changsha 410128, Hunan, Peoples R China.

[Gui, Qingwen; Xu, Zhihui; Jiang, Hongmei] Hunan Univ, Coll Chem & Chem Engn, State Key Lab Chemo Biosensing & Chemometr, Changsha 410082, Hunan, Peoples R China.

[Yu, Xian-Yong] Hunan Univ Sci & Technol, Minist Educ, Key Lab Theoret Organ Chem & Funct Mol, Taoyuan Rd 9, Xiangtan 411201, Peoples R China.

通讯机构：

[Gui, Qingwen] H

Hunan Agr Univ, Coll Sci, Changsha 410128, Hunan, Peoples R China.

Hunan Univ, Coll Chem & Chem Engn, State Key Lab Chemo Biosensing & Chemometr, Changsha 410082, Hunan, Peoples R China.

语种：

英文

期刊：

Organic & Biomolecular Chemistry

ISSN：

1477-0520

年：

2019

卷：

期：

页码：

2715-2720

DOI：

10.1039/c8ob02992j

基金类别：

Hunan Province Science Foundation for Youths [2018JJ3215]; Hunan Agricultural University Science Foundation for High-Level Personnel; National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [31672457]; Local Science and Technology Development Project by the Central Government [YDZX20184300002303]; Ministry of Agriculture of the People's Republic of ChinaMinistry of Agriculture, China [2015-Z64, 2016-X47]; Hunan Provincial Science and Technology Department [2016NK2101, 2016WK2008, 2016TP2005, 2018CT5002]

机构署名：

本校为第一且通讯机构

院系归属：

理学院

摘要：

A simple, practical and metal-free method has been developed for the synthesis of sulfonamides and β-arylsulfonyl enamines via the selective cleavage of C–N and C–H bonds through the iodine-catalyzed oxidation of arenesulfonyl chlorides and sodium sulfinates with tert-amines. The method uses commercially available inexpensive catalysts and oxidants, and has a ...

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TBAI-catalyzed selective synthesis of sulfonamides and β-aryl sulfonyl enamines: coupling of arenesulfonyl chlorides and sodium sulfinates with tert-amines

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