Identification of carbadox metabolites formed by liver microsomes from rats, pigs and chickens using high-performance liquid chromatography combined with hybrid ion trap/time-of-flight mass spectrometry

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成果类型：

期刊论文

作者：

Liu, Zhao-Ying;Tao, Yan-Fei;Chen, Dong-Mei;Wang, Xu;Yuan, Zong-Hui*

通讯作者：

Yuan, Zong-Hui

作者机构：

[Chen, Dong-Mei; Wang, Xu; Liu, Zhao-Ying; Yuan, Zong-Hui; Tao, Yan-Fei] Huazhong Agr Univ, Coll Vet Med, HZAU MAO Key Lab Food Safety Evaluat, Natl Reference Lab Vet Drug Residues, Wuhan 430070, Hubei, Peoples R China.

[Liu, Zhao-Ying] Hunan Agr Univ, Fac Vet, Changsha 410128, Hunan, Peoples R China.

[Yuan, Zong-Hui] Huazhong Agr Univ, Coll Vet Med, HZAU MAO Key Lab Food Safety Evaluat, Natl Reference Lab Vet Drug Residues, Shizishan St, Wuhan 430070, Hubei, Peoples R China.

通讯机构：

[Yuan, Zong-Hui] H

Huazhong Agr Univ, Coll Vet Med, HZAU MAO Key Lab Food Safety Evaluat, Natl Reference Lab Vet Drug Residues, Shizishan St, Wuhan 430070, Hubei, Peoples R China.

语种：

英文

期刊：

Rapid Communications in Mass Spectrometry

ISSN：

0951-4198

年：

2011

卷：

期：

页码：

341-348

DOI：

10.1002/rcm.4833

基金类别：

National Basic Research Program of ChinaNational Basic Research Program of China [2009CB118800]

机构署名：

本校为其他机构

院系归属：

动物医学院

摘要：

Carbadox (methyl-3-(2-quinoxalinylmethylene)-carbazate-N-1, N-4-dioxide) is a chemotherapeutic growth promoter added to feed for starter pigs. In this work, the metabolism of carbadox in rat, pig and chicken liver microsomes has been studied firstly. The incubation mixtures were then processed and analyzed for metabolites with a sensitive and reliable method based on high-performance liquid chromatography combined with hybrid ion trap/time-of-flight mass spectrometry (LC/MS-IT-TOF). With the help of chromatographic behavior and accurate mass measurements, it is possible to rapidly and reliably...

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Identification of carbadox metabolites formed by liver microsomes from rats, pigs and chickens using high-performance liquid chromatography combined with hybrid ion trap/time-of-flight mass spectrometry

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