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Synthesis and Evaluation of Molecularly Imprinted Polymer for the Determination of the Phthalate Esters in the Bottled Beverages by HPLC

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成果类型:
期刊论文
作者:
Jin, Ya-Feng;Zhang, Yi-Jun;Zhang, Yu-Ping*;Chen, Jun;Zhou, Xiao-Mao;...
通讯作者:
Zhang, Yu-Ping
作者机构:
[Jin, Ya-Feng; Zhang, Yi-Jun; Chen, Jun; Zhang, Yu-Ping] Henan Inst Sci & Technol, Xinxiang 453003, Peoples R China.
[Chen, Jun; Bai, Lian-Yang; Zhou, Xiao-Mao] Hunan Agr Univ, Pesticide Res Inst, Changsha 410128, Hunan, Peoples R China.
[Bai, Lian-Yang] Hunan Inst Humanities Sci & Technol, Loudi 417000, Peoples R China.
通讯机构:
[Zhang, Yu-Ping] H
Henan Inst Sci & Technol, Xinxiang 453003, Peoples R China.
语种:
英文
期刊:
Journal of Chemistry
ISSN:
2090-9063
年:
2013
卷:
2013
基金类别:
Scientific Research Foundation for the Returned Overseas Chinese Scholars, State Education MinistryScientific Research Foundation for the Returned Overseas Chinese Scholars; National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [30070506, 30771436]
机构署名:
本校为其他机构
院系归属:
植物保护学院
摘要:
A molecularly imprinted polymer (MIP) was prepared in acetonitrile by bulk polymerization, using di-n-octylphthalate (DOP) as a template molecular, α-methacrylic acid (MAA) as a functional monomer, and ethylene dimethacrylate (EDMA) as a crosslinker. Characterization and evaluation of the prepared MIP were carried out by scanning electron microscope (SEM), infrared absorption spectroscopy (IR), and the Scatchard analysis, respectively. Through the optimization of washing solvent, eluting solvent amount, flow rate of loading solution, and loadi...

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