In this study, an investigation is conducted into the degradation of nitenpyram (NTP) using highly efficient APMMO/PDS/Vis system. As photocatalysts, silver phosphate (AP) and calcined Zn-Al layered double hydroxides (MMO) exhibit high efficiency in achieving charge separation. Besides, the injection of electrons into peroxydisulfate (PDS) from the APMMO can contribute to obtaining the species in the active state with higher efficiency. Based on the APMMO/PDS/Vis system, 50 mg/L of nitenpyram (NTP, 50 mL) can be completely removed in 60 min using 0.8 g/L photocatalyst and 0.2 g/L PDS under the...