期刊论文

中文

饲料研究

1002-2813

2023

46

23

120-125

10.13557/j.cnki.issn1002-2813.2023.23.022

CARS-21:现代农业产业技术体系建设专项资金项目

本校为其他机构

试验旨在建立“槟榔嗜好品”加工过程剩余的槟榔芯的特征图谱。采用高效液相色谱（HPLC）对鲜果槟榔的槟榔芯、实验室模拟工厂的槟榔芯以及工厂提供的22批槟榔芯进行分析，采用ZORBAX 300-SCX色谱柱（4.6 mm×250 mm,5μm），流动相为0.1%磷酸水-乙腈（90∶10）,0.1%磷酸水用三乙胺调pH值为2.30～2.55，等度洗脱，检测波长215 nm，流速1 mL/min，柱温25℃。结果共指认4个特征峰，分别为槟榔碱、槟榔次碱、去甲槟榔碱、去甲槟榔次碱，其中槟榔碱为参照峰（S）。结果显示，上述检测样品中均含有槟榔碱、槟榔次碱、去甲槟榔碱、去甲槟榔次碱，可作为槟榔芯的特征峰，建立的HPLC法精密度、稳定性、重...

The experiment aimed to establish a characteristic chromatogram of the Areca catechu core remaining during the'Areca catechu'processing.Fresh,laboratory simulation of factory conduction and 22 batches of Areca catechu core were analyzed by high performance liquid chromatography(HPLC),ZORBAX 300-SCX column(4.6 mm×250 mm,5 μm)was used,the mobile phase was 0.1%phosphoric acid water-acetonic(90∶10),0.1%phosphoric acid water with amitriptyline pH was 2.30～2.55,the equal elation was carried out,the detection wavelength was 215 nm,the flow rate wa...