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Ultra high performance liquid chromatography with tandem mass spectrometry method for determining dinotefuran and its main metabolites in samples of plants, animal-derived foods, soil, and water

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成果类型:
期刊论文
作者:
Zhang, Ying;Wu, Xiaohu*;Duan, Tingting;Xu, Jun;Dong, Fengshou;...
通讯作者:
Wu, Xiaohu
作者机构:
[Du, Pengqiang; Zheng, Yongquan; Xu, Jun; Dong, Fengshou; Liu, Xingang; Zhang, Ying; Wu, Xiaohu] Chinese Acad Agr Sci, Inst Plant Protect, State Key Lab Biol Plant Dis & Insect Pests, 2 West Yuanmingyuan Rd, Beijing 100193, Peoples R China.
[Zhang, Ying; Duan, Tingting] Guizhou Acad Agr Sci, Inst Plant Protect, Guiyang, Guizhou, Peoples R China.
[Li, Xiaogang; Zhang, Ying] Hunan Agr Univ, Coll Plant Protect, Southern Reg Collaborat Innovat Ctr Grain & Oil C, Changsha, Hunan, Peoples R China.
通讯机构:
[Wu, Xiaohu] C
Chinese Acad Agr Sci, Inst Plant Protect, State Key Lab Biol Plant Dis & Insect Pests, 2 West Yuanmingyuan Rd, Beijing 100193, Peoples R China.
语种:
英文
关键词:
Amines;Animals;Biomolecules;Carbon black;Mass spectrometry;Metabolism;Metabolites;Phase separation;Silica;Solvents;Urea;Zirconia;Dinotefuran;Dispersive solid phase extraction;Environmental sample;Food samples;Solvent effects;Tandem triple quadrupole mass spectrometry;Tetrahydro-3-furylmethyl;Ultra-high performance liquid chromatographies;High performance liquid chromatography;1 methyl 3 (tetrahydro 3 furylmethyl)guanidine;1 methyl 3 (tetrahydro 3 furylmethyl)urea;acetic acid;acetonitrile;amine;black carbon;dinotefuran;guanidine derivative;octadecylsilane;silane derivative;silicon dioxide;unclassified drug;urea derivative;water;zirconium oxide;animal product;animal tissue;Article;controlled study;cost effectiveness analysis;cucumber;egg;limit of quantitation;measurement precision;milk;nonhuman;plant;pork;priority journal;purification;quantitative analysis;residue analysis;rice;soil analysis;solid phase extraction;solvent effect;solvent extraction;tandem mass spectrometry;ultra performance liquid chromatography;validation process;water analysis;watermelon
期刊:
JOURNAL OF SEPARATION SCIENCE
ISSN:
1615-9306
年:
2018
卷:
41
期:
14
页码:
2913-2923
基金类别:
This research was supported by the National Natural Science Foundation of China (31501678 and 31672057).
机构署名:
本校为其他机构
院系归属:
植物保护学院
摘要:
An ultra high-performance liquid chromatography with tandem triple quadrupole mass spectrometry residue method was developed and validated for the quantification and identification of dinotefuran and its main metabolites 1-methyl-3-(tetrahydro-3-furylmethyl) urea and 1-methyl-3-(tetrahydro-3-furylmethyl) guanidine in fruit (watermelon), vegetable (cucumber), cereal (rice), animal-derived foods (milk, egg, and pork), soil, and water. The samples were extracted with acetonitrile containing 15%v/v acetic acid and purified with dispersive solid-pha...

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