In this paper,methyl?β?cyclodextrin was simply synthesized and its impact on the solubilization of methyl?parathion and carbofuran were investigated.The result indicated that methyl?β?cyclodextrin can significantly increase the solubility of parathion?methyl and carbofuran.The concentration of parathion?methyl and carbofuran respectively increased 21.91 and 4.01 times with 20kg/L methyl?β?cyclodextrin.The solubility was linear with concentration of methyl?β?cyclodextrin and matching degree of hydrophobicness molecular geome...