A novel method to quickly prepare molecularly imprinted polymer (MIP) monolithic fibres is developed using microwave irradiation. The well-known water-compatibility problem of MIP is overcome by liquid-liquid-solid microextraction (LLSME). The atrazine (ATR) MIP fibre was obtained after silica was etched away with a controlled length of 1 cm, and subsequently characterized by scanning electron microscopy. Main factors affecting the selective extraction, including extraction time, desorption time, extraction and desorption solvents, were investigated for LLSME procedures in detail. The selectiv...
